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Gas analysis — Preparation of calibration gas mixtures using dynamic volumetric methods — Part 7: Thermal mass-flow controllers
If this method is employed for the preparation of calibration gas mixtures, the optimum performance is as follows: the relative expanded uncertainty of measurement, U, obtained by multiplying the combined standard uncertainty by a coverage factor k = 2, is not greater than 2 %.
If pre-mixed gases are used instead of pure gases, mole fractions below 10-6 can be obtained. The measurement of mass flow is not absolute and the flow controller requires independent calibration.
The merits of the method are that a large quantity of the gas mixture can be prepared on a continuous basis and that multicomponent mixtures can be prepared as readily as binary mixtures if the appropriate number of thermal mass-flow controllers is utilized.
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